纳米二氧化钛光催化剂的研制

李亚男; 林永波

环境保护科学

纳米二氧化钛光催化剂的研制

李亚男, 林永波. 纳米二氧化钛光催化剂的研制[J]. 环境保护科学, 2013, (2): 15-18.

引用本文:

李亚男, 林永波. 纳米二氧化钛光催化剂的研制[J]. 环境保护科学, 2013, (2): 15-18.

LI Ya-nan, LIN Yong-bo . Development of Nano-TiO2 Photocatalyst[J]. Environmental Protection Science, 2013, (2): 15-18.

Citation:

LI Ya-nan, LIN Yong-bo . Development of Nano-TiO₂ Photocatalyst[J]. Environmental Protection Science, 2013, (2): 15-18.

纳米二氧化钛光催化剂的研制

东北林业大学林学院, 黑龙江哈尔滨 150040

作者简介: 李亚男(1985-),女,硕士研究生。研究方向:应用环境学。E-mail:574652287@qq.com

通讯作者: 林永波(1966-),男,副教授

中图分类号: O643.36

Development of Nano-TiO₂ Photocatalyst

Corresponding author: LIN Yong-bo

摘要: 采用溶胶-凝胶法以钛酸四丁酯为钛源、无水乙醇为溶剂、冰醋酸为抑制剂来制备纳米TiO₂光催化剂,通过光催化降解甲基橙水溶液评价体系,根据需要改变实验所用的原料、制备方法和工艺过程,考察蒸馏水、冰醋酸、无水乙醇各因素量对制备的纳米TiO₂催化活性的影响。结果表明当V (钛酸四丁酯):V (冰醋酸):V (蒸馏水):V (无水乙醇)=2:1.2:8:36,脱出率可达到95%以上,为实验条件下纳米TiO₂的最佳制备工艺条件。
- 纳米二氧化钛 /
- 溶胶-凝胶 /
- 光催化
Abstract: This study adopts sol-gel method, with tetrabutyl titanate as the titanium source, anhydrous ethanol as the solvent, glacial acetic acid as inhibitor, to prepare nano-TiO₂ photocatalyst. The effects of distilled water, glacial acetic acid and anhydrous ethanol on the nano-TiO₂ photocatalyst activity are investigated through the evaluation system of photocatalytic degradation of methyl orange solution, according to the raw materials of the different experiments and the preparation methods as well as the process. The results show that the emergence rate can reach more than 95% with V (tetrabutyl titanate):V (glacial acetic acid):V (distilled water):V (anhydrous ethanol)=2:1.2:8:36, and it is the best preparation condition of nano-TiO₂ under the experimental conditions.
- Nano-TiO₂ /
- Sol-Gel /
- Photocatalysis

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李亚男, 林永波. 纳米二氧化钛光催化剂的研制[J]. 环境保护科学, 2013, (2): 15-18.

引用本文:

李亚男, 林永波. 纳米二氧化钛光催化剂的研制[J]. 环境保护科学, 2013, (2): 15-18.

LI Ya-nan, LIN Yong-bo . Development of Nano-TiO2 Photocatalyst[J]. Environmental Protection Science, 2013, (2): 15-18.

Citation:

LI Ya-nan, LIN Yong-bo . Development of Nano-TiO₂ Photocatalyst[J]. Environmental Protection Science, 2013, (2): 15-18.

纳米二氧化钛光催化剂的研制

通讯作者: 林永波(1966-),男,副教授

作者简介: 李亚男(1985-),女,硕士研究生。研究方向:应用环境学。E-mail:574652287@qq.com
东北林业大学林学院, 黑龙江哈尔滨 150040

收稿日期: 2012-11-06

关键词:

摘要: 采用溶胶-凝胶法以钛酸四丁酯为钛源、无水乙醇为溶剂、冰醋酸为抑制剂来制备纳米TiO₂光催化剂,通过光催化降解甲基橙水溶液评价体系,根据需要改变实验所用的原料、制备方法和工艺过程,考察蒸馏水、冰醋酸、无水乙醇各因素量对制备的纳米TiO₂催化活性的影响。结果表明当V (钛酸四丁酯):V (冰醋酸):V (蒸馏水):V (无水乙醇)=2:1.2:8:36,脱出率可达到95%以上,为实验条件下纳米TiO₂的最佳制备工艺条件。

English Abstract

Development of Nano-TiO₂ Photocatalyst

Corresponding author: LIN Yong-bo

Received Date: 2012-11-06

Keywords:

Nano-TiO₂ /
Sol-Gel /
Photocatalysis

Abstract: This study adopts sol-gel method, with tetrabutyl titanate as the titanium source, anhydrous ethanol as the solvent, glacial acetic acid as inhibitor, to prepare nano-TiO₂ photocatalyst. The effects of distilled water, glacial acetic acid and anhydrous ethanol on the nano-TiO₂ photocatalyst activity are investigated through the evaluation system of photocatalytic degradation of methyl orange solution, according to the raw materials of the different experiments and the preparation methods as well as the process. The results show that the emergence rate can reach more than 95% with V (tetrabutyl titanate):V (glacial acetic acid):V (distilled water):V (anhydrous ethanol)=2:1.2:8:36, and it is the best preparation condition of nano-TiO₂ under the experimental conditions.