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凝胶渗透色谱法在分析食品中多氯联苯的应用

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张磊, 李敬光, 赵云峰, 吴永宁. 凝胶渗透色谱法在分析食品中多氯联苯的应用[J]. 环境化学, 2007, 26(2): 197-201.
引用本文: 张磊, 李敬光, 赵云峰, 吴永宁. 凝胶渗透色谱法在分析食品中多氯联苯的应用[J]. 环境化学, 2007, 26(2): 197-201.
shu
ZHANG Lei, LI Jing-guang, ZHAO Yun-feng, WU Yong-ning. APPLICATION OF GEL PERMEATION CHROMATOGRAPHY IN ANALYSIS OF POLYCHLORINATED BIPHENYLS FROM FOOD MATRICES[J]. Environmental Chemistry, 2007, 26(2): 197-201.
Citation: ZHANG Lei, LI Jing-guang, ZHAO Yun-feng, WU Yong-ning. APPLICATION OF GEL PERMEATION CHROMATOGRAPHY IN ANALYSIS OF POLYCHLORINATED BIPHENYLS FROM FOOD MATRICES[J]. Environmental Chemistry, 2007, 26(2): 197-201.
shu

凝胶渗透色谱法在分析食品中多氯联苯的应用

  • 1.

    中国疾病预防控制中心营养与食品安全所, 北京, 100050

  • 基金项目:

    国家重大科技专项《食品安全关键技术》(2002BA804A19)

APPLICATION OF GEL PERMEATION CHROMATOGRAPHY IN ANALYSIS OF POLYCHLORINATED BIPHENYLS FROM FOOD MATRICES

  • 1.

    National Institute for Nutrition and Food Safety, Chinese CDC, Beijing, 100050, China

  • Fund Project:

  • 摘要: 以凝胶渗透色谱(GPC)系统处理食品样品中的脂质,并结合碱性氧化铝柱净化,旨在建立快速有效的多氯联苯(PCBs)分析的前处理技术.对油脂样品的检测结果显示,13C标记PCBs定量内标的回收率及RSD均符合EPA1668a方法的要求,20种天然PCBs的加标回收率在71%-122%,方法精密度≤10%.
    Abstract: To develop a rapid pretreatment technique for determination of polychlorinated biphenyls in food, remove lipid compounds in food stuff effectively, the lipid riched foods were pretreated with gel permeation chromato graphy and then cleaned up using alkali alumina column. Oil samples were analyzed using this method. The results shown that the recovery of 13C labeled PCBs and its RSD well accorded with EPA 1668a method. The recovery of 20 native PCBs were 71%-122%,RSD≤10%.
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  • [1] 李敬光、吴永宁,同位素稀释GC-LRMS 法测定鱼肉中指示性多氯联苯方法研究[J]. 卫生研究,2005,34(3):322-325


    [2] IDF,Milk and Milk Products-Determination of Polychlorinated Biphenyls Guidance on Gas-Liquid Chromatographic Methods[S]. International IDF Standard 130A,1991
    [3] Tuinstra L G M Th,Traag W A,Van J A Rhijn et al.,The Dutch PCB/Dioxin Study Development of a Method for the Determination of Dioxin,Planar and Other PCBs in Human Milk[J]. Chemosphere,1994,29(9-11):1859-1875
    [4] Nerin C,Domeno C,Determination of Polyaromatic Hydrocarbons and Some Related Compounds in Lndustrial Waste Oils by GPC-HPLC-UV[J]. Analyst,1999,124:67-70
    [5] Saito K,Sjodin A,Sandau C D et al.,Development of a Accelerated Solvent Extraction and Gel Permeation Chromatography Analytical Method for Measuring Persistent Organohalogen Compounds in Adipose and Organ Tissue Analysis[J]. Chemosphere,2004,57:373-381

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  • 收稿日期:  2006-09-20
张磊, 李敬光, 赵云峰, 吴永宁. 凝胶渗透色谱法在分析食品中多氯联苯的应用[J]. 环境化学, 2007, 26(2): 197-201.
引用本文: 张磊, 李敬光, 赵云峰, 吴永宁. 凝胶渗透色谱法在分析食品中多氯联苯的应用[J]. 环境化学, 2007, 26(2): 197-201.
shu
ZHANG Lei, LI Jing-guang, ZHAO Yun-feng, WU Yong-ning. APPLICATION OF GEL PERMEATION CHROMATOGRAPHY IN ANALYSIS OF POLYCHLORINATED BIPHENYLS FROM FOOD MATRICES[J]. Environmental Chemistry, 2007, 26(2): 197-201.
Citation: ZHANG Lei, LI Jing-guang, ZHAO Yun-feng, WU Yong-ning. APPLICATION OF GEL PERMEATION CHROMATOGRAPHY IN ANALYSIS OF POLYCHLORINATED BIPHENYLS FROM FOOD MATRICES[J]. Environmental Chemistry, 2007, 26(2): 197-201.
shu

凝胶渗透色谱法在分析食品中多氯联苯的应用

  • 1. 中国疾病预防控制中心营养与食品安全所, 北京, 100050
  • 收稿日期:  2006-09-20
基金项目:

国家重大科技专项《食品安全关键技术》(2002BA804A19)

摘要: 以凝胶渗透色谱(GPC)系统处理食品样品中的脂质,并结合碱性氧化铝柱净化,旨在建立快速有效的多氯联苯(PCBs)分析的前处理技术.对油脂样品的检测结果显示,13C标记PCBs定量内标的回收率及RSD均符合EPA1668a方法的要求,20种天然PCBs的加标回收率在71%-122%,方法精密度≤10%.

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