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一测多评法同时测定嘎日迪-5丸中4种化学成分

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薄彧坤, 郭叶, 康松松, 冯智翱, 杨雪苗, 马瑞寅, 张雨生, 张志勇, 安明, 董志强, 陈丽枝. 一测多评法同时测定嘎日迪-5丸中4种化学成分[J]. 环境化学, 2020, (12): 3585-3587.
引用本文: 薄彧坤, 郭叶, 康松松, 冯智翱, 杨雪苗, 马瑞寅, 张雨生, 张志勇, 安明, 董志强, 陈丽枝. 一测多评法同时测定嘎日迪-5丸中4种化学成分[J]. 环境化学, 2020, (12): 3585-3587.
shu
BO Yukun, GUO Ye, KANG Songsong, FENG Zhiao, YANG Xuemiao, MA Ruiyin, ZHANG Yusheng, ZHANG Zhiyong, AN Ming, DONG Zhiqiang, CHEN Lizhi. Simultaneous determination of 4 chemical constituents in garidi-5 pill by QAMS method[J]. Environmental Chemistry, 2020, (12): 3585-3587.
Citation: BO Yukun, GUO Ye, KANG Songsong, FENG Zhiao, YANG Xuemiao, MA Ruiyin, ZHANG Yusheng, ZHANG Zhiyong, AN Ming, DONG Zhiqiang, CHEN Lizhi. Simultaneous determination of 4 chemical constituents in garidi-5 pill by QAMS method[J]. Environmental Chemistry, 2020, (12): 3585-3587.
shu

一测多评法同时测定嘎日迪-5丸中4种化学成分

  • 1. 包头医学院, 包头, 014040;

  • 2. 包头医学院第一附属医院, 包头, 014010;

  • 3. 岛津企业管理(中国)有限公司, 北京, 100020

    • 通讯作者: 安明, E-mail: 610283014@qq.com ;  董志强, E-mail: dzq4895@163.com ; 
  • 基金项目:

    国家自然科学基金（8521967017）和内蒙古教育厅大学生创新创业训练计划项目（201910127008，201910127011）资助.

Simultaneous determination of 4 chemical constituents in garidi-5 pill by QAMS method

  • 1. Baotou Medical College, Baotou, 014040, China;

  • 2. The First Affiliated Hospital of Baotou Medical College, Baotou, 014010, China;

  • 3. Shimadzu(China) Co., Ltd, Beijing, 100020, China

    • Corresponding authors: AN Ming, 610283014@qq.com ;  DONG Zhiqiang, dzq4895@163.com ; 
  • Fund Project: Supported by the National Natural Science Foundation of China (8521967017) and College Student Innovation and Entrepreneurship Training Program of Inner Mongolia Department of Education(201910127008,201910127011).

  • 摘要: 用HPLC法，以木香烃内酯为内参物，建立该成分与没食子酸、鞣花酸和去氢木香内酯的相对校正因子（fs/i），采用fs/i计算各成分的质量分数.同时以外标法（ESM）测定上述4种化学成分的质量分数，比较两种方法所测含量的差异.结果表明，各相对校正因子重复性良好，RSD值均小于3.0%，嘎日迪-5丸中4种成分采用一测多评法测定结果与外标法测定结果无显著性差异.
    Abstract: With costunolide as the internal reference, the relative correction factors (fs/i) of gallic acid, ellagic acid and dehydrocostus lactone were established by HPLC method, which were used to calculate the content of each component. Meanwhile, the content of 4 chemical constituents were measured by external standard method (ESM). By comparing the content results of the ESM with QAMS, the accuracy and scientificity of QAMS method for quality control of garidi-5 pill were evaluated. The repeatability of fs/i was good,There was no significant difference between the results of QAMS and ESM. the RSD values of the fs/i were less than 3.0%.
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出版历程
薄彧坤, 郭叶, 康松松, 冯智翱, 杨雪苗, 马瑞寅, 张雨生, 张志勇, 安明, 董志强, 陈丽枝. 一测多评法同时测定嘎日迪-5丸中4种化学成分[J]. 环境化学, 2020, (12): 3585-3587.
引用本文: 薄彧坤, 郭叶, 康松松, 冯智翱, 杨雪苗, 马瑞寅, 张雨生, 张志勇, 安明, 董志强, 陈丽枝. 一测多评法同时测定嘎日迪-5丸中4种化学成分[J]. 环境化学, 2020, (12): 3585-3587.
shu
BO Yukun, GUO Ye, KANG Songsong, FENG Zhiao, YANG Xuemiao, MA Ruiyin, ZHANG Yusheng, ZHANG Zhiyong, AN Ming, DONG Zhiqiang, CHEN Lizhi. Simultaneous determination of 4 chemical constituents in garidi-5 pill by QAMS method[J]. Environmental Chemistry, 2020, (12): 3585-3587.
Citation: BO Yukun, GUO Ye, KANG Songsong, FENG Zhiao, YANG Xuemiao, MA Ruiyin, ZHANG Yusheng, ZHANG Zhiyong, AN Ming, DONG Zhiqiang, CHEN Lizhi. Simultaneous determination of 4 chemical constituents in garidi-5 pill by QAMS method[J]. Environmental Chemistry, 2020, (12): 3585-3587.
shu

一测多评法同时测定嘎日迪-5丸中4种化学成分

    通讯作者: 安明, E-mail: 610283014@qq.com ;  董志强, E-mail: dzq4895@163.com ; 
  • 1. 包头医学院, 包头, 014040;
  • 2. 包头医学院第一附属医院, 包头, 014010;
  • 3. 岛津企业管理(中国)有限公司, 北京, 100020
基金项目:

国家自然科学基金（8521967017）和内蒙古教育厅大学生创新创业训练计划项目（201910127008，201910127011）资助.

摘要: 用HPLC法，以木香烃内酯为内参物，建立该成分与没食子酸、鞣花酸和去氢木香内酯的相对校正因子（fs/i），采用fs/i计算各成分的质量分数.同时以外标法（ESM）测定上述4种化学成分的质量分数，比较两种方法所测含量的差异.结果表明，各相对校正因子重复性良好，RSD值均小于3.0%，嘎日迪-5丸中4种成分采用一测多评法测定结果与外标法测定结果无显著性差异.

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